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Registro completo
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Biblioteca (s) : |
INIA Las Brujas. |
Fecha : |
25/10/2014 |
Actualizado : |
03/10/2019 |
Tipo de producción científica : |
Artículos en Revistas Indexadas Internacionales |
Autor : |
NIELL, S.; PAREJA, L.; ASTEGGIANTE, L.G.; ROEHRS, R.; PIZZUTTI, I.R.; GARCIA, C.; HEINZEN, H.; CESIO, M.V. |
Afiliación : |
SILVINA NIELL, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; LUCÍA PAREJA, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; LUCA GEIS ASTEGGIANTE, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; RAFAEL ROEHRS, LARP/Universidade Federal de Santa Maria, Rio Grande do Sul, Brazil.; IONARA R. PIZZUTTI, CEPARC/Universidade Federal de Santa Maria, Rio Grande do Sul, Brazil.; CLAUDIO CESAR GARCIA GALLARRETA, Instituto Nacional de Investigación Agropecuaria (INIA), Uruguay; HORACIO HEINZEN, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay; MARA VERNICA CESIO, Universidad de la República, Farmacognosia y Productos Naturales. Uruguay. |
Título : |
Development of methods for multiresidue analysis of rice post-emergence herbicides in loam soil and their possible applications to soils of different composition. |
Fecha de publicación : |
2010 |
Fuente / Imprenta : |
Journal of AOAC International, 2010, v. 93 no.2, p. 425-431. |
Descripción física : |
2-s2.0-77952781014 |
ISSN : |
1060-3271 |
Idioma : |
Inglés |
Contenido : |
ABSTRACT,
Two simple and straightforward sample preparation methods were developed for the multiresidue analysis of post-emergence herbicides in loam soil that are commonly used in rice crop cultivation. A number of strategic soil extraction and cleanup methods were evaluated. The instrumental analysis was performed by HPLC with a diode array detector. The best compromise between the recoveries (69-98%) and good repeatability (RSD <15%) was obtained using either methanol or methanol-ethyl acetate (70 + 30, v/v) as extraction solvents without any further cleanup. For the first time, residues of metsulfuron methyl, bensulfuron ethyl, bentazone, cyhalofop butyl, pyrazosulfuron ethyl, propanil, and clomazone were analyzed simultaneously. Quinclorac and bispyribac sodium were also assayed, but their recoveries were below 50%. Both methods had an LOD of 0.7 ?g/kg and could accurately determine the residues at the 2 ?g/kg level. These two methods could not be applied directly to other soil types as the recoveries strongly depended on the soil composition. The developed methodologies were successfully applied in monitoring 87 real-world soil samples, in which only propanil (6 to 12 ?g/kg) and clomazone (15 to 20 ?g/kg) residues could be detected. |
Thesagro : |
ANÁLISIS DE SUELOS; ANÁLISIS QUÍMICO; ARROZ; SUELOS. |
Asunto categoría : |
P33 Química y física del suelo |
Marc : |
LEADER 02103naa a2200277 a 4500 001 1051310 005 2019-10-03 008 2010 bl uuuu u00u1 u #d 022 $a1060-3271 100 1 $aNIELL, S. 245 $aDevelopment of methods for multiresidue analysis of rice post-emergence herbicides in loam soil and their possible applications to soils of different composition.$h[electronic resource] 260 $c2010 300 $c2-s2.0-77952781014 520 $aABSTRACT, Two simple and straightforward sample preparation methods were developed for the multiresidue analysis of post-emergence herbicides in loam soil that are commonly used in rice crop cultivation. A number of strategic soil extraction and cleanup methods were evaluated. The instrumental analysis was performed by HPLC with a diode array detector. The best compromise between the recoveries (69-98%) and good repeatability (RSD <15%) was obtained using either methanol or methanol-ethyl acetate (70 + 30, v/v) as extraction solvents without any further cleanup. For the first time, residues of metsulfuron methyl, bensulfuron ethyl, bentazone, cyhalofop butyl, pyrazosulfuron ethyl, propanil, and clomazone were analyzed simultaneously. Quinclorac and bispyribac sodium were also assayed, but their recoveries were below 50%. Both methods had an LOD of 0.7 ?g/kg and could accurately determine the residues at the 2 ?g/kg level. These two methods could not be applied directly to other soil types as the recoveries strongly depended on the soil composition. The developed methodologies were successfully applied in monitoring 87 real-world soil samples, in which only propanil (6 to 12 ?g/kg) and clomazone (15 to 20 ?g/kg) residues could be detected. 650 $aANÁLISIS DE SUELOS 650 $aANÁLISIS QUÍMICO 650 $aARROZ 650 $aSUELOS 700 1 $aPAREJA, L. 700 1 $aASTEGGIANTE, L.G. 700 1 $aROEHRS, R. 700 1 $aPIZZUTTI, I.R. 700 1 $aGARCIA, C. 700 1 $aHEINZEN, H. 700 1 $aCESIO, M.V. 773 $tJournal of AOAC International, 2010$gv. 93 no.2, p. 425-431.
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INIA Las Brujas (LB) |
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Registro completo
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Biblioteca (s) : |
INIA La Estanzuela. |
Fecha actual : |
23/09/2014 |
Actualizado : |
24/04/2017 |
Tipo de producción científica : |
Artículos en Revistas Indexadas Nacionales |
Circulación / Nivel : |
B - 2 |
Autor : |
MENDOZA, A.; LA MANNA, A.; MIERES, J.; ACOSTA, Y. |
Afiliación : |
ALEJANDRO FRANCISCO MENDOZA AGUIAR, Instituto Nacional de Investigación Agropecuaria (INIA), Uruguay; ALEJANDRO FRANCISCO LA MANNA ALONSO, Instituto Nacional de Investigación Agropecuaria (INIA), Uruguay; JUAN MANUEL MIERES VISILLAC, Instituto Nacional de Investigación Agropecuaria (INIA), Uruguay. Investigador fallecido en 2012.; YAMANDU MARTIN ACOSTA AZPIROZ, Instituto Nacional de Investigación Agropecuaria (INIA), Uruguay. |
Título : |
Evaluación del consumo de deoxinivalenol y de un adsorbente comercial de micotoxinas en vacas lecheras a pastoreo. |
Fecha de publicación : |
2014 |
Fuente / Imprenta : |
Agrociencia (Montevideo), v. 18, n. 1, p. 133-140, 2014. |
ISSN : |
2301-1548. |
Idioma : |
Español |
Palabras claves : |
ADSORBENTES DE MIXOTOXINAS; BOVINOS PARA LECHE; CALIDAD DE LECHE; COMPOSICIÓN DE LA LECHE; DEOXINIVALENOL; DON; PRODUCCIÓN DE LECHE; TRICOTECENOS; VACAS LECHERAS. |
Thesagro : |
ALIMENTACIÓN DE RUMIANTES; MICOTOXINAS. |
Asunto categoría : |
L02 Alimentación animal |
URL : |
http://www.ainfo.inia.uy/digital/bitstream/item/5325/1/AGROCIENCIA-v18n1a14.pdf
http://www.scielo.edu.uy/pdf/agro/v18n1/v18n1a14.pdf
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Marc : |
LEADER 00880naa a2200289 a 4500 001 1050469 005 2017-04-24 008 2014 bl uuuu u00u1 u #d 022 $a2301-1548. 100 1 $aMENDOZA, A. 245 $aEvaluación del consumo de deoxinivalenol y de un adsorbente comercial de micotoxinas en vacas lecheras a pastoreo.$h[electronic resource] 260 $c2014 650 $aALIMENTACIÓN DE RUMIANTES 650 $aMICOTOXINAS 653 $aADSORBENTES DE MIXOTOXINAS 653 $aBOVINOS PARA LECHE 653 $aCALIDAD DE LECHE 653 $aCOMPOSICIÓN DE LA LECHE 653 $aDEOXINIVALENOL 653 $aDON 653 $aPRODUCCIÓN DE LECHE 653 $aTRICOTECENOS 653 $aVACAS LECHERAS 700 1 $aLA MANNA, A. 700 1 $aMIERES, J. 700 1 $aACOSTA, Y. 773 $tAgrociencia (Montevideo)$gv. 18, n. 1, p. 133-140, 2014.
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