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| 1. |  | ZANINE, A.M.; RODRIGUEZ MOTTA, J.P.; FERREIRA, D.J.; DE SOUZA, A.L.; RIBEIRO, M.D.; GERON, L.J.V.; FAJARDO, M.; SPRUNK, M.; PINHO, R.M.A. Milk performance and grazing behaviour of dairy cows in response to pasture allowance. Animal Production Science, 2019, Volume 59, Issue 4, Pages 749-756. Article history: Submitted: 26 July 2017 /Accepted: 15 February 2018 / Published online: 14 May 2018.| Biblioteca(s): INIA Las Brujas. |
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 | Acceso al texto completo restringido a Biblioteca INIA Las Brujas. Por información adicional contacte bibliolb@inia.org.uy. |
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Registro completo
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Biblioteca (s) : |
INIA Las Brujas. |
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Fecha actual : |
17/05/2022 |
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Actualizado : |
17/05/2022 |
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Tipo de producción científica : |
Artículos en Revistas Indexadas Internacionales |
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Circulación / Nivel : |
Internacional - -- |
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Autor : |
PALLADINO, C.; MUELA, A.; TABORDA, B.; PUIGVERT, F.; PÉREZ-PARADA, A.; COLAZZO, M.; PÉREZ, C. A.; PEREYRA, S.; PAREJA, L. |
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Afiliación : |
CINTIA PALLADINO, PDU Abordaje Holístico Al Impacto de Los Agroquímicos, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; AGUSTINA MUELA, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; BELÉN TABORDA, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; FLORENCIA PUIGVERT, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay; ANDRÉS PÉREZ-PARADA, Departamento de Desarrollo Tecnológico - DDT, Centro Universitario Regional Del Este, Universidad de la República, Ruta 9 y Ruta 15, 27000, Rocha, Uruguay; MARCOS COLAZZO, Licenciatura en Análisis Alimentario, Inst. Tecnologico Regional Suroeste, Universidad Tecnologica, Calle 17, Saladero Santa Maria, 60000, Paysandu, Uruguay; CARLOS A. PÉREZ, Departamento de Protección Vegetal, Facultad de Agronomía, Universidad de la República, EEMAC, Ruta 3 km 363, Paysandu, 60000, Uruguay; SILVIA ANTONIA PEREYRA CORREA, INIA (Instituto Nacional de Investigación Agropecuaria), Uruguay; LUCÍA PAREJA, Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, 60000, Uruguay. |
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Título : |
Application of a straightforward Mmthodology by LC-QqQ-MS/MS and GC-MS to ensure food safety of barley and wheat grain. |
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Fecha de publicación : |
2022 |
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Fuente / Imprenta : |
ACS Agricultural Science and Technology, 2022, Volume 2, Issue 2, Pages 371-380. doi: https://doi.org/10.1021/acsagscitech.1c00263 |
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ISSN : |
2692-1952 |
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DOI : |
10.1021/acsagscitech.1c00263 |
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Idioma : |
Inglés |
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Notas : |
Article history: Received 29 November 2021; Accepted 24 February 2022; Revised 4 February 2022; Published online 16 March 2022; Published in issue 18 April 2022.
Corresponding author: Pareja, L.; Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, Uruguay; email:lpareja@fq.edu.uy -- |
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Contenido : |
ABSTRACT. A multiclass methodology to determine deoxynivalenol, zearalenone, and 13 widely used fungicides to control the main diseases in barley and wheat crops was optimized and validated. Three QuEChERS methods were compared in terms of recovery and repeatability. The recoveries of the validated method were in the 67-128% range for the selected compounds and relative standard deviations were below 20% according to Document SANTE No. 12682/2019. The limits of quantification (LOQs) were between 10 and 100 μg kg-1. The method was applied for the analysis of barley and wheat grains obtained under production conditions. These samples contained mycotoxins and fungicide residues at concentrations below the LOQs, except for carbendazim in wheat, which exceeded the Codex maximum residue levels. The results of this study provide a fast and simple analytical tool to evaluate the primary production of these grains and to identify possible risks to human health.
© 2022 American Chemical Society. |
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Palabras claves : |
Cereals; Food safety; Fungicide residues; Hyphenated chromatographic techniques; Mycotoxins. |
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Thesagro : |
CEREALES. |
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Asunto categoría : |
F01 Cultivo |
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Marc : |
LEADER 02367naa a2200325 a 4500
001 1063147
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022 $a2692-1952
024 7 $a10.1021/acsagscitech.1c00263$2DOI
100 1 $aPALLADINO, C.
245 $aApplication of a straightforward Mmthodology by LC-QqQ-MS/MS and GC-MS to ensure food safety of barley and wheat grain.$h[electronic resource]
260 $c2022
500 $aArticle history: Received 29 November 2021; Accepted 24 February 2022; Revised 4 February 2022; Published online 16 March 2022; Published in issue 18 April 2022. Corresponding author: Pareja, L.; Departamento de Química Del Litoral, Cenur Litoral Norte, Universidad de la República, Ruta 3 km 363, Paysandu, Uruguay; email:lpareja@fq.edu.uy --
520 $aABSTRACT. A multiclass methodology to determine deoxynivalenol, zearalenone, and 13 widely used fungicides to control the main diseases in barley and wheat crops was optimized and validated. Three QuEChERS methods were compared in terms of recovery and repeatability. The recoveries of the validated method were in the 67-128% range for the selected compounds and relative standard deviations were below 20% according to Document SANTE No. 12682/2019. The limits of quantification (LOQs) were between 10 and 100 μg kg-1. The method was applied for the analysis of barley and wheat grains obtained under production conditions. These samples contained mycotoxins and fungicide residues at concentrations below the LOQs, except for carbendazim in wheat, which exceeded the Codex maximum residue levels. The results of this study provide a fast and simple analytical tool to evaluate the primary production of these grains and to identify possible risks to human health. © 2022 American Chemical Society.
650 $aCEREALES
653 $aCereals
653 $aFood safety
653 $aFungicide residues
653 $aHyphenated chromatographic techniques
653 $aMycotoxins
700 1 $aMUELA, A.
700 1 $aTABORDA, B.
700 1 $aPUIGVERT, F.
700 1 $aPÉREZ-PARADA, A.
700 1 $aCOLAZZO, M.
700 1 $aPÉREZ, C. A.
700 1 $aPEREYRA, S.
700 1 $aPAREJA, L.
773 $tACS Agricultural Science and Technology, 2022, Volume 2, Issue 2, Pages 371-380. doi: https://doi.org/10.1021/acsagscitech.1c00263
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